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Yoneshiro T, Matsushita M, Hibi M, Tone H, Takeshita M, Yasunaga K et al (2017) Tea catechin and caffeine activate brown adipose tissue and increase cold-induced thermogenic capacity in humans

Here we describe the synthesis and kinetic characterization of a fluoromethyl-M(5) analogue that acts as a mechanism-based inhibitor of both enzymes

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For ESI+, the mass spectrometer settings were as follows: capillary voltage of 4500 V, nebulizer gas pressure of 2.0 bar, dry gas flow rate of 10 L min -1 , dry gas temperature of 220C, mass scan range of 50-1300 m/z, spectra acquisition rate of 10 Hz, and cycle time of 0.4 s