For each sample, the amount of radioactivity present was measured on a scintillation counter, and the equal amount of radioactivity was loaded on TLC
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What Meaningful Pinealon Documentation Should Include Identity as Glu-Asp-Arg Complete sequence order Observed intact molecular mass Tandem-MS fragment evidence L-amino-acid stereochemistry Free N-terminal identity Free C-terminal acid identity Pyroglutamate impurity result Aspartimide or isoaspartate assessment Net peptide-content assay Chromatographic purity Free amino-acid results Deletion-sequence results Named and unknown impurities Counterion identification Trifluoroacetate or acetate quantity Water-content result Residual-solvent results Residual synthesis-reagent results Elemental-impurity assessment where relevant pH and appearance Bacterial-endotoxin result Sterility result for a finished injectable medicine Visible and subvisible particle results Batch-specific stability evidence Container-closure compatibility Testing-laboratory identity Analytical methods and acceptance criteria A clear statement identifying tests not performed Why 99% HPLC Is Not Enough HPLC area purity does not prove that the main peak contains Glu-Asp-Arg in the correct order
The American journal of medicine , 20 (6), 896911
