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doi: 10.1210/en.2004-0147

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Detection of CH 4 by GC/MS DMeHg (4 mM) or MeHgCl (4 mM) in 0.5 N HCl-50% methanol was incubated for 3 h or 4 days at room temperature in a glass vial, and then the sample was analyzed by GC/MS