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Sample and instrument details are given with the spectrum Set 1 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz 1: 1D 1H Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz 2: 2D [1H,1H]-TOCSY Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz 3: 1D 13C Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz 4: 1D DEPT90 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz 5: 1D DEPT135 Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz 6: 2D [1H,13C]-HSQC Sample: 100mM in D2O, ref: DSS Conditions: temperature: 298K, pH: 7.4 Spectrometer: Bruker DMX - 400MHz

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